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Figure 7:. Diffraction specimen of synthesized zeolites via various medium temperature (POMFA-KOH=!1:2, P=800 W, f= 45 kHZ and t=2.5h ). increasing of temperature up to 50 °C, the zeolites P appears at 22° 20, and the zeolite X takes place at 50° and 60° 20. The best condition for operation temperature is 80°C.

Figure 7 . Diffraction specimen of synthesized zeolites via various medium temperature (POMFA-KOH=!1:2, P=800 W, f= 45 kHZ and t=2.5h ). increasing of temperature up to 50 °C, the zeolites P appears at 22° 20, and the zeolite X takes place at 50° and 60° 20. The best condition for operation temperature is 80°C.

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The POMFA characterizataion and analysis have been demonstrated. The result of Scanning Microscopic Analysis (SEM) is shown in Figure 1. Figure 1: SEM Micrograph of raw POMFA.
The POMFA characterizataion and analysis have been demonstrated. The result of Scanning Microscopic Analysis (SEM) is shown in Figure 1. Figure 1: SEM Micrograph of raw POMFA.
Figure 3:. FTIR of raw POMFA. FTIR analysis of POMFA is exhibited in the Figure
Figure 3:. FTIR of raw POMFA. FTIR analysis of POMFA is exhibited in the Figure
The raw POMFA has been analyzed by XRD. The XRD pattern of raw POMFA analysis is displayed in Figure 2. which indicated that it consists mainly of amorphous aluminosilicate glass, quartz and mullite.
The raw POMFA has been analyzed by XRD. The XRD pattern of raw POMFA analysis is displayed in Figure 2. which indicated that it consists mainly of amorphous aluminosilicate glass, quartz and mullite.
‘able 1: Major peaks intensity of synthesized zeolites via various ratio of POMFA-KOH. Figure 4 shows the effect of POMFA-KOH ratio
‘able 1: Major peaks intensity of synthesized zeolites via various ratio of POMFA-KOH. Figure 4 shows the effect of POMFA-KOH ratio
Figure 4: Diffraction patterns of synthesized zeolites via various ratio of POMFA-KOH ( T=80°C, P=800 W, f= 45 kHZ and t=2.5h, ). The ratio of POMFA-KOH plays on the zeolites synthesis an important role. The role of POMFA-KOH ratio on the formatted zeolites is shown at Figure 4 and Table 1.
Figure 4: Diffraction patterns of synthesized zeolites via various ratio of POMFA-KOH ( T=80°C, P=800 W, f= 45 kHZ and t=2.5h, ). The ratio of POMFA-KOH plays on the zeolites synthesis an important role. The role of POMFA-KOH ratio on the formatted zeolites is shown at Figure 4 and Table 1.
The ultrasound exposure time effect on the resulted zeolites is reflected at Figure 5 and Table 2.
The ultrasound exposure time effect on the resulted zeolites is reflected at Figure 5 and Table 2.
Table 2: Major peaks intensity of synthesized zeolites via various ultrasound exposure time. The obtained data indicates the highest intensity values at the time of 150 min. (2.5 h). The peak intensity of the synthesized zeolite increases with crystallization time. The ultrasound exposure that is complemented with another reviews and investigations (Pal, et al., 2013; Askari, et al., 2013; Azizi & Asemi, 2014). The highest sum of intensity for ultrasound exposure time is also 150 min. (2.5 h).
Table 2: Major peaks intensity of synthesized zeolites via various ultrasound exposure time. The obtained data indicates the highest intensity values at the time of 150 min. (2.5 h). The peak intensity of the synthesized zeolite increases with crystallization time. The ultrasound exposure that is complemented with another reviews and investigations (Pal, et al., 2013; Askari, et al., 2013; Azizi & Asemi, 2014). The highest sum of intensity for ultrasound exposure time is also 150 min. (2.5 h).
Table 3. Major peaks intensity of synthesized zeolites via various irradiation power. The given data arranges the intensity in XRD powdered pattern with the the highest sum at 800 W. The increasing of ultrasound power influences on the crystallinity of formed zeolites. The ultrasound produces cavitation bubbles with high temperatures and pressures, it results extraordinary heating and cooling rates that develop crystal nuclei. The new formed nuclei overlappes with the presented nuclei that causes the crystal in short time, and the uniform growth of zeolites can be produced (Belviso ef al., 2011). Using all power levels, the zeolites X can be formed and becomes the highest intensity.
Table 3. Major peaks intensity of synthesized zeolites via various irradiation power. The given data arranges the intensity in XRD powdered pattern with the the highest sum at 800 W. The increasing of ultrasound power influences on the crystallinity of formed zeolites. The ultrasound produces cavitation bubbles with high temperatures and pressures, it results extraordinary heating and cooling rates that develop crystal nuclei. The new formed nuclei overlappes with the presented nuclei that causes the crystal in short time, and the uniform growth of zeolites can be produced (Belviso ef al., 2011). Using all power levels, the zeolites X can be formed and becomes the highest intensity.
The irradiation power impact on the manufactured zeolites is demonstrated at Figure 6 and Table 3.
The irradiation power impact on the manufactured zeolites is demonstrated at Figure 6 and Table 3.
The total intensity sum of synthesized zeolites at various temperature is tabulated in Table 4.
The total intensity sum of synthesized zeolites at various temperature is tabulated in Table 4.
Figure 8. GCPOMFAZ SEM images (POMFA- <OH=1:2, T= 80°C, P=800 W, f= 45 KHZ and t=2.5h ). The resulted G-POMFAZ is identified by morphology analysis using SEM. The SEM images is presented at Figure 8.
Figure 8. GCPOMFAZ SEM images (POMFA- <OH=1:2, T= 80°C, P=800 W, f= 45 KHZ and t=2.5h ). The resulted G-POMFAZ is identified by morphology analysis using SEM. The SEM images is presented at Figure 8.
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